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Microstructure and Fracture Toughness of an Extruded Mg-Dy-Nd-Zn-Zr Alloy Influenced by Heat Treatment

Research output: Contributions to collected editions/works › Article in conference proceedings › Research › peer-review

Standard

Microstructure and Fracture Toughness of an Extruded Mg-Dy-Nd-Zn-Zr Alloy Influenced by Heat Treatment. / Maier, Petra; Clausius, Benjamin; Joy, Charis et al.
Magnesium Technology 2021. ed. / Victoria M. Miller; Petra Maier; J. Brian Jordon; Neale R. Neelameggham. Cham: Springer Science and Business Media Deutschland, 2021. p. 19-26 (Minerals, Metals and Materials Series).

Research output: Contributions to collected editions/works › Article in conference proceedings › Research › peer-review

Harvard

Maier, P, Clausius, B, Joy, C, Menze, R, Bittner, B & Hort, N 2021, Microstructure and Fracture Toughness of an Extruded Mg-Dy-Nd-Zn-Zr Alloy Influenced by Heat Treatment. in VM Miller, P Maier, JB Jordon & NR Neelameggham (eds), Magnesium Technology 2021. Minerals, Metals and Materials Series, Springer Science and Business Media Deutschland, Cham, pp. 19-26, Magnesium Technology Symposium held at the 150th TMS Annual Meeting and Exhibition - TMS 2021, Virtual, Online, 15.03.21. https://doi.org/10.1007/978-3-030-65528-0_4

APA

Maier, P., Clausius, B., Joy, C., Menze, R., Bittner, B., & Hort, N. (2021). Microstructure and Fracture Toughness of an Extruded Mg-Dy-Nd-Zn-Zr Alloy Influenced by Heat Treatment. In V. M. Miller, P. Maier, J. B. Jordon, & N. R. Neelameggham (Eds.), Magnesium Technology 2021 (pp. 19-26). (Minerals, Metals and Materials Series). Springer Science and Business Media Deutschland. https://doi.org/10.1007/978-3-030-65528-0_4

Vancouver

Maier P, Clausius B, Joy C, Menze R, Bittner B, Hort N. Microstructure and Fracture Toughness of an Extruded Mg-Dy-Nd-Zn-Zr Alloy Influenced by Heat Treatment. In Miller VM, Maier P, Jordon JB, Neelameggham NR, editors, Magnesium Technology 2021. Cham: Springer Science and Business Media Deutschland. 2021. p. 19-26. (Minerals, Metals and Materials Series). doi: 10.1007/978-3-030-65528-0_4

Bibtex

@inbook{d37c8794ef2948049d8d12215cfc1e4b,
title = "Microstructure and Fracture Toughness of an Extruded Mg-Dy-Nd-Zn-Zr Alloy Influenced by Heat Treatment",
abstract = "The influence of microstructural changes induced by heat treatment on fracture toughness is investigated for a resorbable Mg-Dy based alloy. The initial hot-extruded condition is a fine-grained Resoloy{\textregistered} (Mg–Dy–Nd–Zn–Zr) alloy consisting of lamellar LPSO structures within the matrix. Solution heat treatment causes grain growth and the formation of blocky LPSO phases. The amount of the lamellar LPSO structures reduces. Quasi-static C-ring tests with and without Ringer solution were used to evaluate force–displacement curves and their fracture energy. The coarser-grained alloys tend to twin under plastic deformation, which is influencing the crack propagation. Blocky LPSO phases clearly hinder crack growth. The fine-grained extruded condition shows the highest force and displacement values to induce the crack, the solution heat-treated microstructure consisting of a good balance of grain size, matrix, and blocky LPSO phases and twins show highest fracture energy. Even if there might be an absorption of hydrogen, the ductility under stress corrosion is high.",
keywords = "Crack propagation, Fracture toughness, LPSO phases, Magnesium, RESOLOY{\textregistered}, Engineering",
author = "Petra Maier and Benjamin Clausius and Charis Joy and Roman Menze and Benjamin Bittner and Norbert Hort",
year = "2021",
doi = "10.1007/978-3-030-65528-0_4",
language = "English",
isbn = "978-3-030-65527-3",
series = "Minerals, Metals and Materials Series",
publisher = "Springer Science and Business Media Deutschland",
pages = "19--26",
editor = "Miller, {Victoria M.} and Petra Maier and Jordon, {J. Brian} and Neelameggham, {Neale R.}",
booktitle = "Magnesium Technology 2021",
address = "Germany",
note = "Magnesium Technology Symposium held at the 150th TMS Annual Meeting and Exhibition - TMS 2021, TMS2021 ; Conference date: 15-03-2021 Through 18-03-2021",
url = "https://www.tms.org/TMS2021/Programming/TMS2021_Proceedings_Information/TMS2021/Programming/TMS2021_Proceedings_Information.aspx?hkey=336d34e8-27fe-42a2-85c6-6e5256e1b9d1",

}

RIS

TY - CHAP

T1 - Microstructure and Fracture Toughness of an Extruded Mg-Dy-Nd-Zn-Zr Alloy Influenced by Heat Treatment

AU - Maier, Petra

AU - Clausius, Benjamin

AU - Joy, Charis

AU - Menze, Roman

AU - Bittner, Benjamin

AU - Hort, Norbert

N1 - Conference code: 150

PY - 2021

Y1 - 2021

N2 - The influence of microstructural changes induced by heat treatment on fracture toughness is investigated for a resorbable Mg-Dy based alloy. The initial hot-extruded condition is a fine-grained Resoloy® (Mg–Dy–Nd–Zn–Zr) alloy consisting of lamellar LPSO structures within the matrix. Solution heat treatment causes grain growth and the formation of blocky LPSO phases. The amount of the lamellar LPSO structures reduces. Quasi-static C-ring tests with and without Ringer solution were used to evaluate force–displacement curves and their fracture energy. The coarser-grained alloys tend to twin under plastic deformation, which is influencing the crack propagation. Blocky LPSO phases clearly hinder crack growth. The fine-grained extruded condition shows the highest force and displacement values to induce the crack, the solution heat-treated microstructure consisting of a good balance of grain size, matrix, and blocky LPSO phases and twins show highest fracture energy. Even if there might be an absorption of hydrogen, the ductility under stress corrosion is high.

AB - The influence of microstructural changes induced by heat treatment on fracture toughness is investigated for a resorbable Mg-Dy based alloy. The initial hot-extruded condition is a fine-grained Resoloy® (Mg–Dy–Nd–Zn–Zr) alloy consisting of lamellar LPSO structures within the matrix. Solution heat treatment causes grain growth and the formation of blocky LPSO phases. The amount of the lamellar LPSO structures reduces. Quasi-static C-ring tests with and without Ringer solution were used to evaluate force–displacement curves and their fracture energy. The coarser-grained alloys tend to twin under plastic deformation, which is influencing the crack propagation. Blocky LPSO phases clearly hinder crack growth. The fine-grained extruded condition shows the highest force and displacement values to induce the crack, the solution heat-treated microstructure consisting of a good balance of grain size, matrix, and blocky LPSO phases and twins show highest fracture energy. Even if there might be an absorption of hydrogen, the ductility under stress corrosion is high.

KW - Crack propagation

KW - Fracture toughness

KW - LPSO phases

KW - Magnesium

KW - RESOLOY®

KW - Engineering

UR - http://www.scopus.com/inward/record.url?scp=85102752839&partnerID=8YFLogxK

U2 - 10.1007/978-3-030-65528-0_4

DO - 10.1007/978-3-030-65528-0_4

M3 - Article in conference proceedings

AN - SCOPUS:85102752839

SN - 978-3-030-65527-3

T3 - Minerals, Metals and Materials Series

SP - 19

EP - 26

BT - Magnesium Technology 2021

A2 - Miller, Victoria M.

A2 - Maier, Petra

A2 - Jordon, J. Brian

A2 - Neelameggham, Neale R.

PB - Springer Science and Business Media Deutschland

CY - Cham

T2 - Magnesium Technology Symposium held at the 150th TMS Annual Meeting and Exhibition - TMS 2021

Y2 - 15 March 2021 through 18 March 2021

ER -

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Exploring the degradation behavior of biodegradable metals (Mg, Zn, and Fe) in human duodenal fluid

Zhang, Y., Cao, J., Liu, H., Wang, C., Chu, C., Xue, F., Willumeit-Römer, R., Hort, N., Huang, Y. & Bai, J., 05.2025, In: Journal of Magnesium and Alloys. 13, 5, p. 2103-2119 17 p.

Research output: Journal contributions › Journal articles › Research › peer-review

Insight into the self-healing performance of dicalcium phosphate dihydrate coating on magnesium wires: Its damage and anti-corrosive behavior under deformation

Zhang, Y., Nie, T., Chen, D., Jiang, G., Xu, W., Liu, H., Qian, K., Ju, J., Chu, C., Xue, F., Huang, Y., Hort, N. & Bai, J., 09.2025, In: Corrosion Science. 254, 17 p., 113051.

Research output: Journal contributions › Journal articles › Research › peer-review

Microstructure-Oriented Fatigue Crack Propagation in Two Cast Mg–Al–Ba–Ca Alloys

Maier, P., Wolfram, B., Roggelin, J. & Hort, N., 2025, Magnesium Technology 2025. Tolnai, D., Palumbo, A., Leonard, A. & Neelameggham, N. R. (eds.). Springer Science and Business Media Deutschland, p. 87-96 10 p. (Minerals, Metals and Materials Series).

Research output: Contributions to collected editions/works › Article in conference proceedings › Research › peer-review

The Role of Geometry in Mg Implant Design

Hort, N., Wiese, B., Witte, F. & Maier, P., 2025, Magnesium Technology 2025. Tolnai, D., Palumbo, A., Leonard, A. & Neelameggham, N. R. (eds.). Cham: Springer Science and Business Media Deutschland, p. 3-8 6 p. (Minerals, Metals and Materials Series).

Research output: Contributions to collected editions/works › Article in conference proceedings › Research › peer-review

Utilizing Synchrotron Radiation for Phase Identification in Mg Alloys

Szakács, G., Tolnai, D., Wiese, B. & Hort, N., 2025, TMS 2025 154th Annual Meeting and Exhibition Supplemental Proceedings. Cham: Springer Nature, p. 1587-1599 13 p. (The Minerals, Metals and Materials Series).

Research output: Contributions to collected editions/works › Article in conference proceedings › Research › peer-review

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