Elution of monomers from provisional composite materials
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In: International Journal of Polymer Science, Vol. 2015, 617407, 01.01.2015.
Research output: Journal contributions › Journal articles › Research › peer-review
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TY - JOUR
T1 - Elution of monomers from provisional composite materials
AU - Schulz, Simon Daniel
AU - Laquai, Tobias
AU - Kümmerer, Klaus
AU - Bolek, Richard
AU - Mersch-Sundermann, Volker
AU - Polydorou, Olga
PY - 2015/1/1
Y1 - 2015/1/1
N2 - The aim of this study was to evaluate the elution of substances from different materials used for the manufacturing of temporary indirect restorations, after storage in saliva and ethanol 75%. 10 samples of three chemically cured materials (Protemp 3 Garant, Systemp.c&b, and Trim) and one light-cured material (Clip F) were stored in saliva and ethanol 75% for 24 h, 7, and days 28 days. From the storage media at each time period, samples were prepared and analysed by LC-MS/MS, in order to access the elution of monomers. The results differed among the materials (P ≤ 0.05). No monomers were detected in the samples of Protemp 3 Garant and Clip F. Substances were detected only in ethanol samples of Systemp.c&b and Trim. The amount of BisGMA, TEGDMA, and UDMA 2 released from Systemp.c&b was higher compared to Trim. Storage time affected the release of substances (P ≤ 0.05). The highest release was observed within the first 24 h. It can be concluded that provisional resin composite materials do not show high release of monomers and this release is material dependent. However, the detection of additional peaks during the analysis, suggesting the formation of by-products of the eluted substances, may not be in favour of these materials with respect to their toxicity.
AB - The aim of this study was to evaluate the elution of substances from different materials used for the manufacturing of temporary indirect restorations, after storage in saliva and ethanol 75%. 10 samples of three chemically cured materials (Protemp 3 Garant, Systemp.c&b, and Trim) and one light-cured material (Clip F) were stored in saliva and ethanol 75% for 24 h, 7, and days 28 days. From the storage media at each time period, samples were prepared and analysed by LC-MS/MS, in order to access the elution of monomers. The results differed among the materials (P ≤ 0.05). No monomers were detected in the samples of Protemp 3 Garant and Clip F. Substances were detected only in ethanol samples of Systemp.c&b and Trim. The amount of BisGMA, TEGDMA, and UDMA 2 released from Systemp.c&b was higher compared to Trim. Storage time affected the release of substances (P ≤ 0.05). The highest release was observed within the first 24 h. It can be concluded that provisional resin composite materials do not show high release of monomers and this release is material dependent. However, the detection of additional peaks during the analysis, suggesting the formation of by-products of the eluted substances, may not be in favour of these materials with respect to their toxicity.
KW - Chemistry
UR - http://www.scopus.com/inward/record.url?scp=84926618040&partnerID=8YFLogxK
U2 - 10.1155/2015/617407
DO - 10.1155/2015/617407
M3 - Journal articles
AN - SCOPUS:84926618040
VL - 2015
JO - International Journal of Polymer Science
JF - International Journal of Polymer Science
SN - 1687-9422
M1 - 617407
ER -