SBSE-GC-ECD/FPD in the analysis of pesticide residues in Passiflora alata Dryander herbal teas

Research output: Journal contributionsJournal articlesResearchpeer-review

Authors

  • Carlo Bicchi
  • Chiara Cordero
  • Cristina Iori
  • Patrizia Rubiolo
  • Pat Sandra
  • Janete H. Yariwake
  • Vania G. Zuin

Stir bar sorptive extraction (SBSE) in combination with GC-ECD/FPD analysis is here applied to the determination of the residues of 11 pesticides (hexachlorobenzene, lindane, chlorothalonil, parathion methyl, parathion ethyl, fenitrothion, malathion, dieldrin, α- and β-endosulfan, and tetradifon) in herbal teas prepared with Passiflora alata Dryander spiked leaves. The method was optimized using spiked herbal teas in a range from 0.05 to 1 pg/μL for organochlorine pesticides and from 0.15 to 3 pg/μL for organophosphorus pesticides. The method is reproducible and repeatable with recoveries calculated from herbal teas prepared with spiked plant material versus spiked herbal teas, varying from about 30% for tetradifon to about 90% for parathion methyl and malathion. The limits of quantitation (LOQs) ranged from 0.017 pg/μL for lindane to 0.117 pg/μL for malathion.

Original languageEnglish
JournalJournal of Agricultural and Food Chemistry
Volume51
Issue number1
Pages (from-to)27-33
Number of pages7
ISSN0021-8561
DOIs
Publication statusPublished - 01.01.2003
Externally publishedYes

    Research areas

  • Herbal teas, Medicinal plants, Passiflora alata Dryander, Pesticide residues, Sample preparation, Stir bar sorptive extraction (SBSE)
  • Chemistry

DOI

Recently viewed

Publications

  1. High quality extrudates from aluminum chips by new billet compaction and deformation routes
  2. Urbanes Lernen. Stadt als vielfältiges Lern- und Erfahrungsfeld - aus Sicht einer Stadtplanerin
  3. Mit Film- und Hausarbeit gegen die Kapitalisierung von Zeit (Jeanne Dielman und Fannie Drayton)
  4. Zur Vereinbarkeit rationalistischer und kulturalistischer Ansätze in der Politikwissenschaft
  5. Das Wahlsystem zwischen normativer Begründung, empirischer Evidenz und politischen Interessen
  6. Zur "Paradoxie" der sozialpädagogischen Diskussion um Sozialraumorientierung in der Jugendhilfe
  7. An Empirical Investigation of Terrorism-Induced Stress on Expatriate Attitudes and Performance
  8. You'll better stay at home?- Studies on the Recreational Effects of Holidays and Holiday Tourism
  9. Das Sozialmanagement stärken: Qualitätskriterien und Nutzwertanalyse im Corporate Volunteering
  10. Determinants of entrepreneurial intent: A meta-analytic test and integration of competing models
  11. Wasserverschmutzung im grenzübergreifenden Einzugsgebiet des Zarafshan Flusses in Zentralasien
  12. Blick über den Zaun: Leseförderung in Europa. Ergebnisse und Einsichten aus dem EU-Projekt ADORE
  13. Ein quantitativer Vergleich der subjektiven und objektiven Komplexität von Verkehrssituationen
  14. IWRM through WFD implementation? Drivers for integration in polycentric water governance systems
  15. TextGraphs 2024 Shared Task on Text-Graph Representations for Knowledge Graph Question Answering
  16. Patients' experiences in a guided Internet- and App-based stress intervention for college students
  17. Climate and large-sized trees, but not diversity, drive above-ground biomass in subtropical forests