Crystal structures of 1-2-(dicyclohexylphosphinophenyl)pyrol-2- dicyclohexylphosphino-rhodium(I) norborna-2,5-diene tetrafluoroborate tetrahydrofuran hemisolvate, [Rh(C 34H 5INP 2)(C 7H 8)] [BF 4] · 0.5C 4H 8O, and 1-2-(dicyclohexylphosphinophenyl)-pyrol-2- dicyclohexylphosphino-rhodium(I) (Z,Z)-cycloocta...
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In: Zeitschrift für Kristallographie, Vol. 222, No. 4, 01.12.2007, p. 458-462.
Research output: Journal contributions › Journal articles › Research › peer-review
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TY - JOUR
T1 - Crystal structures of 1-2-(dicyclohexylphosphinophenyl)pyrol-2- dicyclohexylphosphino-rhodium(I) norborna-2,5-diene tetrafluoroborate tetrahydrofuran hemisolvate, [Rh(C 34H 5INP 2)(C 7H 8)] [BF 4] · 0.5C 4H 8O, and 1-2-(dicyclohexylphosphinophenyl)-pyrol-2- dicyclohexylphosphino-rhodium(I) (Z,Z)-cycloocta...
AU - Jackstell, Ralf
AU - Dai, Zhenya
AU - Schmidt, Thomas
AU - Heller, Detlef
AU - Drexler, Hans-Joachim
PY - 2007/12/1
Y1 - 2007/12/1
N2 - Title full: Crystal structures of 1-2-(dicyclohexylphosphinophenyl)pyrol-2- dicyclohexylphosphino-rhodium(I) norborna-2,5-diene tetrafluoroborate tetrahydrofuran hemisolvate, [Rh(C 34H 5INP 2)(C 7H 8)] [BF 4] · 0.5C 4H 8O, and 1-2-(dicyclohexylphosphinophenyl)-pyrol-2- dicyclohexylphosphino-rhodium(I) (Z,Z)-cycloocta-1,5-diene tetrafluoroborate, [Rh(C 34H 5INP 2)(C 8H 12)] [BF 4]. C 43H 63BF 4NO 0.50P 2 Rh, monoclinic, P12 1/n1 (no. 14), a = 10.341(2) Å, b = 16.063(3) Å, c = 27.425(5) Å, β = 98.76(3)°, V= 4502.4 Å 3, Z = 4, R gt(F) = 0.060, wR ref(F 2) = 0.143, T = 200 K. C 42H 63BF 4NP 2Rh, monoclinic, P12 1/c1 (no. 14), a = 10.503(2) Å, b = 17.665(4) Å, c = 21.946(4) Å, β = 101.95(3)°, V= 3983.5 Å 3, Z = 4, R gt(F) = 0.045, wR ref(F 2) = 0.013, T =200 K.
AB - Title full: Crystal structures of 1-2-(dicyclohexylphosphinophenyl)pyrol-2- dicyclohexylphosphino-rhodium(I) norborna-2,5-diene tetrafluoroborate tetrahydrofuran hemisolvate, [Rh(C 34H 5INP 2)(C 7H 8)] [BF 4] · 0.5C 4H 8O, and 1-2-(dicyclohexylphosphinophenyl)-pyrol-2- dicyclohexylphosphino-rhodium(I) (Z,Z)-cycloocta-1,5-diene tetrafluoroborate, [Rh(C 34H 5INP 2)(C 8H 12)] [BF 4]. C 43H 63BF 4NO 0.50P 2 Rh, monoclinic, P12 1/n1 (no. 14), a = 10.341(2) Å, b = 16.063(3) Å, c = 27.425(5) Å, β = 98.76(3)°, V= 4502.4 Å 3, Z = 4, R gt(F) = 0.060, wR ref(F 2) = 0.143, T = 200 K. C 42H 63BF 4NP 2Rh, monoclinic, P12 1/c1 (no. 14), a = 10.503(2) Å, b = 17.665(4) Å, c = 21.946(4) Å, β = 101.95(3)°, V= 3983.5 Å 3, Z = 4, R gt(F) = 0.045, wR ref(F 2) = 0.013, T =200 K.
KW - Chemistry
UR - http://www.scopus.com/inward/record.url?scp=42149105641&partnerID=8YFLogxK
UR - https://www.mendeley.com/catalogue/deb64e34-f7cc-3780-a4c5-a2c63987d935/
U2 - 10.1524/ncrs.2007.0194
DO - 10.1524/ncrs.2007.0194
M3 - Journal articles
VL - 222
SP - 458
EP - 462
JO - Zeitschrift für Kristallographie
JF - Zeitschrift für Kristallographie
SN - 0044-2968
SN - 2196-7105
IS - 4
ER -