Crystal structures of 1-2-(dicyclohexylphosphinophenyl)pyrol-2- dicyclohexylphosphino-rhodium(I) norborna-2,5-diene tetrafluoroborate tetrahydrofuran hemisolvate, [Rh(C 34H 5INP 2)(C 7H 8)] [BF 4] · 0.5C 4H 8O, and 1-2-(dicyclohexylphosphinophenyl)-pyrol-2- dicyclohexylphosphino-rhodium(I) (Z,Z)-cycloocta...

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@article{301fd72c2b944cb58a77c4b920064787,
title = "Crystal structures of 1-2-(dicyclohexylphosphinophenyl)pyrol-2- dicyclohexylphosphino-rhodium(I) norborna-2,5-diene tetrafluoroborate tetrahydrofuran hemisolvate, [Rh(C 34H 5INP 2)(C 7H 8)] [BF 4] · 0.5C 4H 8O, and 1-2-(dicyclohexylphosphinophenyl)-pyrol-2- dicyclohexylphosphino-rhodium(I) (Z,Z)-cycloocta...",
abstract = "Title full: Crystal structures of 1-2-(dicyclohexylphosphinophenyl)pyrol-2- dicyclohexylphosphino-rhodium(I) norborna-2,5-diene tetrafluoroborate tetrahydrofuran hemisolvate, [Rh(C 34H 5INP 2)(C 7H 8)] [BF 4] · 0.5C 4H 8O, and 1-2-(dicyclohexylphosphinophenyl)-pyrol-2- dicyclohexylphosphino-rhodium(I) (Z,Z)-cycloocta-1,5-diene tetrafluoroborate, [Rh(C 34H 5INP 2)(C 8H 12)] [BF 4]. C 43H 63BF 4NO 0.50P 2 Rh, monoclinic, P12 1/n1 (no. 14), a = 10.341(2) {\AA}, b = 16.063(3) {\AA}, c = 27.425(5) {\AA}, β = 98.76(3)°, V= 4502.4 {\AA} 3, Z = 4, R gt(F) = 0.060, wR ref(F 2) = 0.143, T = 200 K. C 42H 63BF 4NP 2Rh, monoclinic, P12 1/c1 (no. 14), a = 10.503(2) {\AA}, b = 17.665(4) {\AA}, c = 21.946(4) {\AA}, β = 101.95(3)°, V= 3983.5 {\AA} 3, Z = 4, R gt(F) = 0.045, wR ref(F 2) = 0.013, T =200 K.",
keywords = "Chemistry",
author = "Ralf Jackstell and Zhenya Dai and Thomas Schmidt and Detlef Heller and Hans-Joachim Drexler",
year = "2007",
month = dec,
day = "1",
doi = "10.1524/ncrs.2007.0194",
language = "English",
volume = "222",
pages = "458--462",
journal = "Zeitschrift f{\"u}r Kristallographie",
issn = "0044-2968",
publisher = "Walter de Gruyter GmbH",
number = "4",

}

RIS

TY - JOUR

T1 - Crystal structures of 1-2-(dicyclohexylphosphinophenyl)pyrol-2- dicyclohexylphosphino-rhodium(I) norborna-2,5-diene tetrafluoroborate tetrahydrofuran hemisolvate, [Rh(C 34H 5INP 2)(C 7H 8)] [BF 4] · 0.5C 4H 8O, and 1-2-(dicyclohexylphosphinophenyl)-pyrol-2- dicyclohexylphosphino-rhodium(I) (Z,Z)-cycloocta...

AU - Jackstell, Ralf

AU - Dai, Zhenya

AU - Schmidt, Thomas

AU - Heller, Detlef

AU - Drexler, Hans-Joachim

PY - 2007/12/1

Y1 - 2007/12/1

N2 - Title full: Crystal structures of 1-2-(dicyclohexylphosphinophenyl)pyrol-2- dicyclohexylphosphino-rhodium(I) norborna-2,5-diene tetrafluoroborate tetrahydrofuran hemisolvate, [Rh(C 34H 5INP 2)(C 7H 8)] [BF 4] · 0.5C 4H 8O, and 1-2-(dicyclohexylphosphinophenyl)-pyrol-2- dicyclohexylphosphino-rhodium(I) (Z,Z)-cycloocta-1,5-diene tetrafluoroborate, [Rh(C 34H 5INP 2)(C 8H 12)] [BF 4]. C 43H 63BF 4NO 0.50P 2 Rh, monoclinic, P12 1/n1 (no. 14), a = 10.341(2) Å, b = 16.063(3) Å, c = 27.425(5) Å, β = 98.76(3)°, V= 4502.4 Å 3, Z = 4, R gt(F) = 0.060, wR ref(F 2) = 0.143, T = 200 K. C 42H 63BF 4NP 2Rh, monoclinic, P12 1/c1 (no. 14), a = 10.503(2) Å, b = 17.665(4) Å, c = 21.946(4) Å, β = 101.95(3)°, V= 3983.5 Å 3, Z = 4, R gt(F) = 0.045, wR ref(F 2) = 0.013, T =200 K.

AB - Title full: Crystal structures of 1-2-(dicyclohexylphosphinophenyl)pyrol-2- dicyclohexylphosphino-rhodium(I) norborna-2,5-diene tetrafluoroborate tetrahydrofuran hemisolvate, [Rh(C 34H 5INP 2)(C 7H 8)] [BF 4] · 0.5C 4H 8O, and 1-2-(dicyclohexylphosphinophenyl)-pyrol-2- dicyclohexylphosphino-rhodium(I) (Z,Z)-cycloocta-1,5-diene tetrafluoroborate, [Rh(C 34H 5INP 2)(C 8H 12)] [BF 4]. C 43H 63BF 4NO 0.50P 2 Rh, monoclinic, P12 1/n1 (no. 14), a = 10.341(2) Å, b = 16.063(3) Å, c = 27.425(5) Å, β = 98.76(3)°, V= 4502.4 Å 3, Z = 4, R gt(F) = 0.060, wR ref(F 2) = 0.143, T = 200 K. C 42H 63BF 4NP 2Rh, monoclinic, P12 1/c1 (no. 14), a = 10.503(2) Å, b = 17.665(4) Å, c = 21.946(4) Å, β = 101.95(3)°, V= 3983.5 Å 3, Z = 4, R gt(F) = 0.045, wR ref(F 2) = 0.013, T =200 K.

KW - Chemistry

UR - http://www.scopus.com/inward/record.url?scp=42149105641&partnerID=8YFLogxK

UR - https://www.mendeley.com/catalogue/deb64e34-f7cc-3780-a4c5-a2c63987d935/

U2 - 10.1524/ncrs.2007.0194

DO - 10.1524/ncrs.2007.0194

M3 - Journal articles

VL - 222

SP - 458

EP - 462

JO - Zeitschrift für Kristallographie

JF - Zeitschrift für Kristallographie

SN - 0044-2968

SN - 2196-7105

IS - 4

ER -

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