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Study of the solidification of AS alloys combining in situ synchrotron diffraction and differential scanning calorimetry

Research output: Contributions to collected editions/works › Article in conference proceedings › Research › peer-review

Standard

Study of the solidification of AS alloys combining in situ synchrotron diffraction and differential scanning calorimetry. / Tolnai, Domonkos; Szakács, Gábor; Requena, Guillermo et al.
Light Metals Technology 2013. ed. / Ian Stone; Brian McKay; Zhongyun Fan. Trans Tech Publications Ltd, 2013. p. 286-290 (Materials Science Forum; Vol. 765).

Research output: Contributions to collected editions/works › Article in conference proceedings › Research › peer-review

Harvard

Tolnai, D, Szakács, G, Requena, G, Stark, A, Schell, N, Kainer, KU & Hort, N 2013, Study of the solidification of AS alloys combining in situ synchrotron diffraction and differential scanning calorimetry. in I Stone, B McKay & Z Fan (eds), Light Metals Technology 2013. Materials Science Forum, vol. 765, Trans Tech Publications Ltd, pp. 286-290, 6th International Light Metals Technology Conference - LMT 2013, Old Windsor, United Kingdom, 24.07.13. https://doi.org/10.4028/www.scientific.net/MSF.765.286

APA

Tolnai, D., Szakács, G., Requena, G., Stark, A., Schell, N., Kainer, K. U., & Hort, N. (2013). Study of the solidification of AS alloys combining in situ synchrotron diffraction and differential scanning calorimetry. In I. Stone, B. McKay, & Z. Fan (Eds.), Light Metals Technology 2013 (pp. 286-290). (Materials Science Forum; Vol. 765). Trans Tech Publications Ltd. https://doi.org/10.4028/www.scientific.net/MSF.765.286

Vancouver

Tolnai D, Szakács G, Requena G, Stark A, Schell N, Kainer KU et al. Study of the solidification of AS alloys combining in situ synchrotron diffraction and differential scanning calorimetry. In Stone I, McKay B, Fan Z, editors, Light Metals Technology 2013. Trans Tech Publications Ltd. 2013. p. 286-290. (Materials Science Forum). doi: 10.4028/www.scientific.net/MSF.765.286

Bibtex

@inbook{78a6db3fbb8647e294732549c623e45c,
title = "Study of the solidification of AS alloys combining in situ synchrotron diffraction and differential scanning calorimetry",
abstract = "In situ synchrotron diffraction experiments were performed during Differential Scanning Calorimetry (DSC) of AS31, AS33 and AS35 alloys. The samples were encapsulated in stainless steel crucibles during the measurement using an empty crucible as the reference. The samples were heated up to 680°C, melted and solidified in the beginning of the experiment in order to fill the crucible. This short cycle was followed by three subsequent cycles between 400°C and 680°C with 5, 10 and 20 K/min heating and cooling rates with 5 min of holding time in the molten state. The diffraction patterns were recorded every 6 s during the DSC program by a Perkin-Elmer XRD 1622 Flatpanel detector including an acquisition time of 3 s and the collection of reference images. The endothermic and exothermic peaks are in correlation with the dissolution and formation of new diffraction patterns, respectively. During cooling from the liquid state, first, α-Mg dendrites solidify, followed by the formation of Mg2Si and Mg17Al12 intermetallics. The results are correlated with those obtained by thermodynamic simulations performed with the software Pandat.",
keywords = "Differential scanning calorimetry, In situ synchrotron diffraction, Mg-Al-Si alloys, Engineering",
author = "Domonkos Tolnai and G{\'a}bor Szak{\'a}cs and Guillermo Requena and Andreas Stark and Norbert Schell and Kainer, {Karl U.} and Norbert Hort",
year = "2013",
month = jul,
day = "1",
doi = "10.4028/www.scientific.net/MSF.765.286",
language = "English",
isbn = "9783037857663",
series = "Materials Science Forum",
publisher = "Trans Tech Publications Ltd",
pages = "286--290",
editor = "Ian Stone and Brian McKay and Zhongyun Fan",
booktitle = "Light Metals Technology 2013",
address = "Switzerland",
note = "6th International Light Metals Technology Conference - LMT 2013, LMT2013 ; Conference date: 24-07-2013 Through 26-07-2013",

}

RIS

TY - CHAP

T1 - Study of the solidification of AS alloys combining in situ synchrotron diffraction and differential scanning calorimetry

AU - Tolnai, Domonkos

AU - Szakács, Gábor

AU - Requena, Guillermo

AU - Stark, Andreas

AU - Schell, Norbert

AU - Kainer, Karl U.

AU - Hort, Norbert

N1 - Conference code: 6

PY - 2013/7/1

Y1 - 2013/7/1

N2 - In situ synchrotron diffraction experiments were performed during Differential Scanning Calorimetry (DSC) of AS31, AS33 and AS35 alloys. The samples were encapsulated in stainless steel crucibles during the measurement using an empty crucible as the reference. The samples were heated up to 680°C, melted and solidified in the beginning of the experiment in order to fill the crucible. This short cycle was followed by three subsequent cycles between 400°C and 680°C with 5, 10 and 20 K/min heating and cooling rates with 5 min of holding time in the molten state. The diffraction patterns were recorded every 6 s during the DSC program by a Perkin-Elmer XRD 1622 Flatpanel detector including an acquisition time of 3 s and the collection of reference images. The endothermic and exothermic peaks are in correlation with the dissolution and formation of new diffraction patterns, respectively. During cooling from the liquid state, first, α-Mg dendrites solidify, followed by the formation of Mg2Si and Mg17Al12 intermetallics. The results are correlated with those obtained by thermodynamic simulations performed with the software Pandat.

AB - In situ synchrotron diffraction experiments were performed during Differential Scanning Calorimetry (DSC) of AS31, AS33 and AS35 alloys. The samples were encapsulated in stainless steel crucibles during the measurement using an empty crucible as the reference. The samples were heated up to 680°C, melted and solidified in the beginning of the experiment in order to fill the crucible. This short cycle was followed by three subsequent cycles between 400°C and 680°C with 5, 10 and 20 K/min heating and cooling rates with 5 min of holding time in the molten state. The diffraction patterns were recorded every 6 s during the DSC program by a Perkin-Elmer XRD 1622 Flatpanel detector including an acquisition time of 3 s and the collection of reference images. The endothermic and exothermic peaks are in correlation with the dissolution and formation of new diffraction patterns, respectively. During cooling from the liquid state, first, α-Mg dendrites solidify, followed by the formation of Mg2Si and Mg17Al12 intermetallics. The results are correlated with those obtained by thermodynamic simulations performed with the software Pandat.

KW - Differential scanning calorimetry

KW - In situ synchrotron diffraction

KW - Mg-Al-Si alloys

KW - Engineering

UR - http://www.scopus.com/inward/record.url?scp=84882962500&partnerID=8YFLogxK

UR - https://www.mendeley.com/catalogue/1bda2c76-0cc5-3a74-bb02-19a7ad0e6974/

U2 - 10.4028/www.scientific.net/MSF.765.286

DO - 10.4028/www.scientific.net/MSF.765.286

M3 - Article in conference proceedings

AN - SCOPUS:84882962500

SN - 9783037857663

T3 - Materials Science Forum

SP - 286

EP - 290

BT - Light Metals Technology 2013

A2 - Stone, Ian

A2 - McKay, Brian

A2 - Fan, Zhongyun

PB - Trans Tech Publications Ltd

T2 - 6th International Light Metals Technology Conference - LMT 2013

Y2 - 24 July 2013 through 26 July 2013

ER -

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Zhang, Y., Cao, J., Liu, H., Wang, C., Chu, C., Xue, F., Willumeit-Römer, R., Hort, N., Huang, Y. & Bai, J., 05.2025, In: Journal of Magnesium and Alloys. 13, 5, p. 2103-2119 17 p.

Research output: Journal contributions › Journal articles › Research › peer-review

Insight into the self-healing performance of dicalcium phosphate dihydrate coating on magnesium wires: Its damage and anti-corrosive behavior under deformation

Zhang, Y., Nie, T., Chen, D., Jiang, G., Xu, W., Liu, H., Qian, K., Ju, J., Chu, C., Xue, F., Huang, Y., Hort, N. & Bai, J., 09.2025, In: Corrosion Science. 254, 17 p., 113051.

Research output: Journal contributions › Journal articles › Research › peer-review

Microstructure-Oriented Fatigue Crack Propagation in Two Cast Mg–Al–Ba–Ca Alloys

Maier, P., Wolfram, B., Roggelin, J. & Hort, N., 2025, Magnesium Technology 2025. Tolnai, D., Palumbo, A., Leonard, A. & Neelameggham, N. R. (eds.). Springer Science and Business Media Deutschland, p. 87-96 10 p. (Minerals, Metals and Materials Series).

Research output: Contributions to collected editions/works › Article in conference proceedings › Research › peer-review

The Role of Geometry in Mg Implant Design

Hort, N., Wiese, B., Witte, F. & Maier, P., 2025, Magnesium Technology 2025. Tolnai, D., Palumbo, A., Leonard, A. & Neelameggham, N. R. (eds.). Cham: Springer Science and Business Media Deutschland, p. 3-8 6 p. (Minerals, Metals and Materials Series).

Research output: Contributions to collected editions/works › Article in conference proceedings › Research › peer-review

Utilizing Synchrotron Radiation for Phase Identification in Mg Alloys

Szakács, G., Tolnai, D., Wiese, B. & Hort, N., 2025, TMS 2025 154th Annual Meeting and Exhibition Supplemental Proceedings. Cham: Springer Nature, p. 1587-1599 13 p. (The Minerals, Metals and Materials Series).

Research output: Contributions to collected editions/works › Article in conference proceedings › Research › peer-review

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