Influence of heat treatment on microstructure of hot extruded AZ31

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Influence of heat treatment on microstructure of hot extruded AZ31. / Dzwonczyk, J.; Bohlen, J.; Hort, Norbert et al.

In: Materials Science Forum, Vol. 419-422, No. I, 01.03.2003, p. 297-302.

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Dzwonczyk J, Bohlen J, Hort N, Kainer KU. Influence of heat treatment on microstructure of hot extruded AZ31. Materials Science Forum. 2003 Mar 1;419-422(I):297-302. doi: 10.4028/www.scientific.net/msf.419-422.297

Bibtex

@article{ca6a5ee9ce1840859b84b3ee6a1d3f58,
title = "Influence of heat treatment on microstructure of hot extruded AZ31",
abstract = "In the last years magnesium alloys have been increasingly considered as attractive materials for the transportation industry. Extruded magnesium alloys have been found in the centre of interest combining their lightweight, surface quality with the wide range of possible achievable geometries. In the present study the alloy AZ31 has been chosen for investigation as one of the most common commercial magnesium wrought alloys. Round bars have been obtained through hot direct extrusion. After primary microstructural characterisation and mechanical testing in the as-extruded condition the specimens have been subjected to heat treatment consisting of different times (1, 2 and 4 hours) at different temperatures (200°C, 300°C, 400°C and 500°C) followed by cooling in air. Subsequently the specimens have been subjected to microstructural characterisation using light optical microscopy. Average grain size and grain size distribution have been determined using dedicated software. The microstructural analysis has been supported by microhardness testing on selected specimens. Additionally, the specimens have been subjected to tensile tests at room temperature applying a deformation rate of 1.3 × 10-4 s-1 as used for the material in as-extruded conditions. The obtained results have shown that heat treatment has no substantial influence on the microstructure characteristics of AZ31 up to 400°C. However, specimens treated at 500°C for one hour revealed a course grain, homogeneous structure with a substantial increase in grain size from 8 μm in as-extruded condition to 18 μm. This change in microstructure slightly reduced the strain-hardening exponent from 0.2 to 0.16. The remaining mechanical properties did not vary extensively when compared to the untreated, as-extruded material. It is assumed that the average grain size and grain size distribution have been influenced by complex thermomechanical treatments, which occurred during extrusion process as well as during heat treatment after heating at 500°C. By controlling the condition of heat treatment it is possible to improve the homogeneity of the material.",
keywords = "AZ31 alloy, Grain size distribution, Heat treatment, Microstructure, Engineering",
author = "J. Dzwonczyk and J. Bohlen and Norbert Hort and Kainer, {K. U.}",
year = "2003",
month = mar,
day = "1",
doi = "10.4028/www.scientific.net/msf.419-422.297",
language = "English",
volume = "419-422",
pages = "297--302",
journal = "Materials Science Forum",
issn = "0255-5476",
publisher = "Trans Tech Publications",
number = "I",
note = "Second Osaka International Conference on Platform Science and Technology for Advanced Magnesium Alloys 2003 ; Conference date: 26-01-2003 Through 30-01-2003",

}

RIS

TY - JOUR

T1 - Influence of heat treatment on microstructure of hot extruded AZ31

AU - Dzwonczyk, J.

AU - Bohlen, J.

AU - Hort, Norbert

AU - Kainer, K. U.

N1 - Conference code: 2

PY - 2003/3/1

Y1 - 2003/3/1

N2 - In the last years magnesium alloys have been increasingly considered as attractive materials for the transportation industry. Extruded magnesium alloys have been found in the centre of interest combining their lightweight, surface quality with the wide range of possible achievable geometries. In the present study the alloy AZ31 has been chosen for investigation as one of the most common commercial magnesium wrought alloys. Round bars have been obtained through hot direct extrusion. After primary microstructural characterisation and mechanical testing in the as-extruded condition the specimens have been subjected to heat treatment consisting of different times (1, 2 and 4 hours) at different temperatures (200°C, 300°C, 400°C and 500°C) followed by cooling in air. Subsequently the specimens have been subjected to microstructural characterisation using light optical microscopy. Average grain size and grain size distribution have been determined using dedicated software. The microstructural analysis has been supported by microhardness testing on selected specimens. Additionally, the specimens have been subjected to tensile tests at room temperature applying a deformation rate of 1.3 × 10-4 s-1 as used for the material in as-extruded conditions. The obtained results have shown that heat treatment has no substantial influence on the microstructure characteristics of AZ31 up to 400°C. However, specimens treated at 500°C for one hour revealed a course grain, homogeneous structure with a substantial increase in grain size from 8 μm in as-extruded condition to 18 μm. This change in microstructure slightly reduced the strain-hardening exponent from 0.2 to 0.16. The remaining mechanical properties did not vary extensively when compared to the untreated, as-extruded material. It is assumed that the average grain size and grain size distribution have been influenced by complex thermomechanical treatments, which occurred during extrusion process as well as during heat treatment after heating at 500°C. By controlling the condition of heat treatment it is possible to improve the homogeneity of the material.

AB - In the last years magnesium alloys have been increasingly considered as attractive materials for the transportation industry. Extruded magnesium alloys have been found in the centre of interest combining their lightweight, surface quality with the wide range of possible achievable geometries. In the present study the alloy AZ31 has been chosen for investigation as one of the most common commercial magnesium wrought alloys. Round bars have been obtained through hot direct extrusion. After primary microstructural characterisation and mechanical testing in the as-extruded condition the specimens have been subjected to heat treatment consisting of different times (1, 2 and 4 hours) at different temperatures (200°C, 300°C, 400°C and 500°C) followed by cooling in air. Subsequently the specimens have been subjected to microstructural characterisation using light optical microscopy. Average grain size and grain size distribution have been determined using dedicated software. The microstructural analysis has been supported by microhardness testing on selected specimens. Additionally, the specimens have been subjected to tensile tests at room temperature applying a deformation rate of 1.3 × 10-4 s-1 as used for the material in as-extruded conditions. The obtained results have shown that heat treatment has no substantial influence on the microstructure characteristics of AZ31 up to 400°C. However, specimens treated at 500°C for one hour revealed a course grain, homogeneous structure with a substantial increase in grain size from 8 μm in as-extruded condition to 18 μm. This change in microstructure slightly reduced the strain-hardening exponent from 0.2 to 0.16. The remaining mechanical properties did not vary extensively when compared to the untreated, as-extruded material. It is assumed that the average grain size and grain size distribution have been influenced by complex thermomechanical treatments, which occurred during extrusion process as well as during heat treatment after heating at 500°C. By controlling the condition of heat treatment it is possible to improve the homogeneity of the material.

KW - AZ31 alloy

KW - Grain size distribution

KW - Heat treatment

KW - Microstructure

KW - Engineering

UR - http://www.scopus.com/inward/record.url?scp=19244370136&partnerID=8YFLogxK

U2 - 10.4028/www.scientific.net/msf.419-422.297

DO - 10.4028/www.scientific.net/msf.419-422.297

M3 - Conference article in journal

AN - SCOPUS:19244370136

VL - 419-422

SP - 297

EP - 302

JO - Materials Science Forum

JF - Materials Science Forum

SN - 0255-5476

IS - I

T2 - Second Osaka International Conference on Platform Science and Technology for Advanced Magnesium Alloys 2003

Y2 - 26 January 2003 through 30 January 2003

ER -