In situ synchrotron radiation diffraction during solidification of Mg4Y and Mg4YxGd alloys (x - 1, 4 wt.%)
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Magnesium Technology 2014 - Held During TMS 2014 143rd Annual Meeting and Exhibition. Hrsg. / Martyn Alderman; Michele V. Manuel; Nobert Hort; Neale R. Neelameggham. The Minerals, Metals & Materials Society, 2014. S. 213-218 (Magnesium Technology).
Publikation: Beiträge in Sammelwerken › Aufsätze in Konferenzbänden › Forschung › begutachtet
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TY - CHAP
T1 - In situ synchrotron radiation diffraction during solidification of Mg4Y and Mg4YxGd alloys (x - 1, 4 wt.%)
AU - Szakacs, G.
AU - Wiese, B.
AU - Mendis, C. L.
AU - Tolnai, D.
AU - Stark, A.
AU - Schell, N.
AU - Naira, M.
AU - Kainer, K. U.
AU - Hort, N.
N1 - Conference code: 143
PY - 2014
Y1 - 2014
N2 - Mg-RE alloys have potential to be used for bio-applications as degradable implant materials. For the production of these alloys casting plays an important role: Phase formation and microstructure evolution are at first determined during solidification. In situ synchrotron radiation diffraction is a unique tool to follow phase formation, phase transformations and grain growth during solidification. The measurements were performed at the High Energy Materials Science beamline P07 at PETRA III at the Deutsches Elektronen-Synchrotron (DESY, Hamburg, Germany). In the present study Mg4Y, Mg4YlGd and Mg4Y4Gd alloys were investigated to characterize their solidification behavior during cooling from 800°C and 680°C to 450°C, respectively with a cooling rate of 20 K/min. The samples were held in graphite crucibles and were molten in a modified Bahr 805 dilatometer under Ar atmosphere, while the temperature was controlled by type S thermocouples. The results are compared with thermodynamic simulations using Pandat 8™ software.
AB - Mg-RE alloys have potential to be used for bio-applications as degradable implant materials. For the production of these alloys casting plays an important role: Phase formation and microstructure evolution are at first determined during solidification. In situ synchrotron radiation diffraction is a unique tool to follow phase formation, phase transformations and grain growth during solidification. The measurements were performed at the High Energy Materials Science beamline P07 at PETRA III at the Deutsches Elektronen-Synchrotron (DESY, Hamburg, Germany). In the present study Mg4Y, Mg4YlGd and Mg4Y4Gd alloys were investigated to characterize their solidification behavior during cooling from 800°C and 680°C to 450°C, respectively with a cooling rate of 20 K/min. The samples were held in graphite crucibles and were molten in a modified Bahr 805 dilatometer under Ar atmosphere, while the temperature was controlled by type S thermocouples. The results are compared with thermodynamic simulations using Pandat 8™ software.
KW - In situ solidification
KW - Mg-RE alloys
KW - Phase formation
KW - Synchrotron diffraction
KW - Engineering
UR - http://www.scopus.com/inward/record.url?scp=84899854557&partnerID=8YFLogxK
U2 - 10.1002/9781118888179.ch42
DO - 10.1002/9781118888179.ch42
M3 - Article in conference proceedings
AN - SCOPUS:84899854557
SN - 9781118888162
T3 - Magnesium Technology
SP - 213
EP - 218
BT - Magnesium Technology 2014 - Held During TMS 2014 143rd Annual Meeting and Exhibition
A2 - Alderman, Martyn
A2 - Manuel, Michele V.
A2 - Hort, Nobert
A2 - Neelameggham, Neale R.
PB - The Minerals, Metals & Materials Society
T2 - 143rd Annual Meeting and Exhibition of Magnesium Technology 2014 - TMS 2014
Y2 - 16 February 2014 through 20 February 2014
ER -