As solidified microstructure investigation of Mg15Y and MgxYyGd (x+y=15 wt.%) ternary alloys
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Magnesium Technology 2016 - Held During TMS 2016: 145th Annual Meeting and Exhibition. Hrsg. / Alok Singh; Kiran Solanki; Michele Viola Manuel; Neale R. Neelameggham. The Minerals, Metals & Materials Society, 2016. S. 23-27 (Magnesium Technology; Band 2016-January).
Publikation: Beiträge in Sammelwerken › Aufsätze in Konferenzbänden › Forschung › begutachtet
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T1 - As solidified microstructure investigation of Mg15Y and MgxYyGd (x+y=15 wt.%) ternary alloys
AU - Szakács, G.
AU - Mendis, C. L.
AU - Tolnai, D.
AU - Vlcek, M.
AU - Lukác, F.
AU - Stulíková, I.
AU - Smola, B.
AU - Wolff, M.
AU - Schmid-Fetzer, R.
AU - Schell, N.
AU - Kainer, K. U.
AU - Hort, N.
N1 - Conference code: 145
PY - 2016
Y1 - 2016
N2 - MgxYyGd (x+y=15 wt.%) alloys were produced via permanent mould casting to investigate the microstructure evolution during solidification of the ternary system. The microstructure of the as-solidified samples was characterized with scanning electron microscopy (SEM) and transmission electron microscopy (TEM). In situ synchrotron radiation diffraction experiments were performed during the solidification of the alloys at the P07 (HEMS) Beamline of PETRA III at DESY. The phase evolution observed during controlled cooling at 20 and 100 K/min and the resultant microstructures were compared with the as-cast conditions. The experimental results were correlated with the calculations from the Pandat thermodynamic software. In the case of the ternary alloys the equilibrium phase diagram suggests the formation of the Mg24Y5 phase at elevated temperatures followed by the formation of the Mg5Gd phase at eutectic temperatures. However, the experiment shows only the formation of Mg24Y5 phase at eutectic temperatures even with a cooling rate (CR) of 100 K/min.
AB - MgxYyGd (x+y=15 wt.%) alloys were produced via permanent mould casting to investigate the microstructure evolution during solidification of the ternary system. The microstructure of the as-solidified samples was characterized with scanning electron microscopy (SEM) and transmission electron microscopy (TEM). In situ synchrotron radiation diffraction experiments were performed during the solidification of the alloys at the P07 (HEMS) Beamline of PETRA III at DESY. The phase evolution observed during controlled cooling at 20 and 100 K/min and the resultant microstructures were compared with the as-cast conditions. The experimental results were correlated with the calculations from the Pandat thermodynamic software. In the case of the ternary alloys the equilibrium phase diagram suggests the formation of the Mg24Y5 phase at elevated temperatures followed by the formation of the Mg5Gd phase at eutectic temperatures. However, the experiment shows only the formation of Mg24Y5 phase at eutectic temperatures even with a cooling rate (CR) of 100 K/min.
KW - In situ synchrotron radiation diffraction
KW - Mg-RE alloys
KW - Microstructures
KW - Phase formation
KW - Solidification
KW - Engineering
UR - http://www.scopus.com/inward/record.url?scp=84975038263&partnerID=8YFLogxK
U2 - 10.1007/978-3-319-48114-2_7
DO - 10.1007/978-3-319-48114-2_7
M3 - Article in conference proceedings
AN - SCOPUS:84975038263
T3 - Magnesium Technology
SP - 23
EP - 27
BT - Magnesium Technology 2016 - Held During TMS 2016
A2 - Singh, Alok
A2 - Solanki, Kiran
A2 - Manuel, Michele Viola
A2 - Neelameggham, Neale R.
PB - The Minerals, Metals & Materials Society
T2 - 145th Annual Meeting and Exhibition of Magnesium Technology - TMS 2016
Y2 - 14 February 2016 through 18 February 2016
ER -